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Efficient Preparations of Fluorine Compounds

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ISBN-10: 111807856X

ISBN-13: 9781118078563

Edition: 2013

Authors: Herbert W. Roesky, Karl Barry Sharpless

List price: $137.00
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Description:

This book brings together contributions written by leading researchers and covering a wide scope of fluorine chemistry. It is a comprehensive listing of methods for synthesizing fluorine compounds for a wide variety of compounds whereby the C-H bond is replaced by a C-F bond. 
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Book details

List price: $137.00
Copyright year: 2013
Publisher: John Wiley & Sons, Incorporated
Publication date: 11/6/2012
Binding: Hardcover
Pages: 484
Size: 6.25" wide x 9.50" long x 1.00" tall
Weight: 1.782
Language: English

Foreword
Preface
Contributors
Preparation of Elemental Fluorine
Preparation of Highly Active Caesium Fluoride
Preparation of Highly Active Silver Fluoride
A Room Temperature, Non-Irradiative Synthesis of Xenon Difluoride (XeF2)
Efficient Perfluorination of K2B12H12 in Neutralizing Acetonitrile
Efficient Preparation of the Highly Soluble ortho- and para-C60(CF2C6F5)2 Derivatives
Synthesis of Cs[1-H-CB11F11]
Synthesis of Zero-Valent Trifluoromethyl Chalcogenato Derivatives, [NMe4]ECF3 (E = S, Se, Te) and Related Compounds
Synthesis Methods for Exotic Inorganic Fluorides with Varied Applications
Tris(pentafluorophenyl)boran, B(C6F5)3, a Powerful, Well-soluble, and Non-oxidizing Lewis Acid and the Weakly Coordinating Tetrakis(pentafluorophenyl)borate Anion, [B(C6F5)4]?
Pentafluorophenyldifluoroboran, C6F5BF2, and Pentafluorophenyltrifluorosilane, C6F5SiF3, Versatile Reagents for Fluorine/Pentafluorophenyl Substitution Reactions in Strongly Oxidizing Hypervalent Non-metal Fluorides
Iodine(III and V) Fluorides: Interesting Fluorinating Agents
Tetramethylammonium Fluoride, [N(CH3)4]F, a Widely Applicable Reagent to Introduce Fluoride Ions and a Suitable Nucleophile to Initiate the Transfer of Perfluoroorganyl Groups to Electrophiles� Hermann-Josef Frohn
Preparation of Transition Metal Sulfide Fluorides
Transition Metal Carbonyl Sulfur Dioxide and Thiazylfluoride Complexes: Reactions at the Metal Center and at the Ligand
Cesium-, Mercury- and Silver-Salts with Sulfur-Nitrogen-Fluorine Anions: Useful Transfer-Reagents for NSF-Building Blocks
Laboratory-Scale Synthesis of Gold Trifluoride and Uranium Hexafluoride
Preparation of Fluorine Containing Molecular Halides and Hetero polar Salts with Elements of Group 15 and Niobium and Tantalum Halides
Fluoro- and Fluorohydroxy Complexes of As, Sb, and Sn
Trifluoromethyl Compounds via Electrophilic and Nucleophilic Reactions
Introduction of Fluorine into Compounds via Electrophilic and Nucleophilic Reactions
The ?Real? Iodine and Bromine Mono-Fluorides
The Versatile Chemistry of Acetyl Hypofluorite ?� Hypofluorite not Bonded to Polyhaloalkyl group� Shlomo Rozen
The Surprising Chemistry of Bromine Trifluoride
Preparation of Silicon- and Sulfur-Based Fluorinated Methane Derivatives as Versatile Fluoromethylation Reagents
Pentafluoroethyl Lithium: Reactions with Carbonyl Compounds and Epoxides
Synthesis of ?-hydroxy-�,�-difluoromethylenephosphonates
Synthesis of Pentafluoro-?6-sulfanyl Substituted Acetylenes for Liquid Crystals
Delocalized Lipophilic Cations as a Source of Naked Fluoride and Phase-transfer Catalysts
Methyltrifluoropyruvate Imines Possessing N-oxalyl and N-phosphonoformyl Groups ? Precursors to a Variety of �-CF3-�-amino Acid Derivatives
Rhodium-mediated Synthesis of (3,3,3-Trifluoropropyl)trimethoxysilane and (3,3,3 trifluoropropyl)triphenylsilane
Rhodium-mediated Synthesis of a Tetrafluoropyridyl-2-boronate Ester
Palladium-mediated Synthesis of 4-Vinyltetrafluoropyridine and 2,3,5,6-Tetrafluoropyridine
Preparation of Polyfluoroaryl-1,2-difluorovinylsilanes
Preparation of (Z)-2-iodo-1,2-difluorostyrenes
Preparation of 1,4-Bis(Z-2-iodo-1,2-difluoroethenyl)benzene
Stereospecific Carboamidation Route to (Z)-N-Phenyl-2,3-difluoro-3-(triethylsilyl) acrylamide
Preparation of 2-Trifluoromethyl-3,3,3-trifluoropropanal
Synthesis of Tetrafluorocatechol
Preparation of an Unsymmetrial Bis((perfluoroalkyl)sulfonyl)imide
Preparation of Perfluoroalkyl Sulfilimines and Sulfoximines
Preparation of Trifluoromethylsulfonium Salts
Preparation of Organometallic Fluorides of Main Group and Transition Elements
Preparation of Pentafluorosulfanyl Carbonyl Compounds
Synthesis of Fluorine Containing Heterocycles from �,�-Dihydropolyfluoroalkylsulfides and Fluorinated Thiocarboxylic Acids
Synthesis of Octafluorocyclooctatetraene
Preparation of Fluoroolefins
Preparation of Ionic Liquids of Fluorocomplex and Oxofluorocomplex Anions by Fluoroacid-base Reactions
Synthesis of Difluorocyclopropyl Building Blocks:� 2,2-Difluorocyclopropylmethanol and 2-(Bromomethyl)-1,1-Difluorocyclopropane
Preparation of 1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane and Perfluoro[2.2]paracyclophane
Efficient Preparation of Bioorganic Fluorine Compounds
1,3-Dipolar Cycloaddition Reactions to Fluoroalkenes
Synthesis of Fluorinated Vinyl Derivatives of Nucleic Acid Bases
Synthesis of CF3-substituted Aziridine Ring by the Gabriel Reaction
Preparation of �-Fluoro Amino and �-Fluoro Enamino Reagents
Synthesis of Original Fluoromonomers and Their Radical copolymerization with Vinylidene fluoride
Convergent 18F Radiosynthesis
Asymmetric Fluorocyclization Reactions
Preparation of Allylic Fluorides
Dehydroxyfluorinations of Primary or Secondary Alcohols Using Perfluoro n-butylsulfonyl Fluoride (nonaflyl Fluoride, NfF) in Combination with 1,8-Diaza-bicyclo[5.4.0]undec-7-ene (DBU)
Preparation of Rare Earth Fluorosulfides� and Oxyfluorosulfides
Preparation of Carbon-Fluorine Compounds and Fluoride or Oxide Fluoride-Intercalated Graphites
Safe Synthesis of Superstoichiometric Mesoporous Fluorocarbons
Preparation of Fluorinated ?-Alumina
Index