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NMR and Chemistry An Introduction to Modern NMR Spectroscopy, Fourth Edition

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ISBN-10: 0748743448

ISBN-13: 9780748743445

Edition: 4th 2000 (Revised)

Authors: J. W. Akitt, B E Mann

List price: $89.95
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Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the…    
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Book details

List price: $89.95
Edition: 4th
Copyright year: 2000
Publisher: CRC Press LLC
Publication date: 2/17/2000
Binding: Paperback
Pages: 400
Size: 7.36" wide x 9.65" long x 0.94" tall
Weight: 1.628

Preface to the fourth edition
The theory of nuclear magnetization
The properties of the nucleus of an atom
The nucleus in a magnetic field
The source of the NMR signal
A basic NMR spectrometer
The magnetic field at the nucleus: nuclear screening and the chemical shift
Effects due to the molecule
Isotope effects
Effects due to unpaired electrons
The chemical shift
Notes on sample preparation, standardization and solvent and temperature effects
Internuclear spin-spin coupling
The mutual effects of nuclear magnets on resonance positions
The appearance of multiplets arising from spin-spin coupling
Spin-spin coupling satellites
The description of spin systems
Second-order effects
Nuclear magnetic relaxation
Relaxation processes in assemblies of nuclear spins
Dipole-dipole relaxation
Quadrupolar relaxation
Spin rotation relaxation: detailed molecular motion
Chemical shift anisotropy relaxation
Scalar relaxation
Examples of [superscript 13]C relaxation times
The spectrometer
The magnet and field homogeneity
The probe
Field-frequency lock
The transmitter
The detection system
Production of the spectrum
Rapid multiple pulsing
Manipulation of collected data
Making the spins dance
Composite pulses
Refocusing pulse
NMR spectra of exchanging and reacting systems
Systems at equilibrium
Reaction monitoring of systems not at equilibrium
Multiple resonance and one-dimensional pulse sequences
Decoupling difference spectroscopy
The nuclear Overhauser effect
One-dimensional multipulse sequences
Exercises in spectral interpretation
Two-dimensional NMR spectroscopy
J-resolved two-dimensional NMR spectroscopy
Homonuclear COSY NMR spectroscopy
Heteronuclear COSY NMR spectroscopy
Two-dimensional Inadequate
Overhauser and magnetization transfer based two-dimensional NMR spectroscopy
Inverse detection
Three-dimensional NMR spectroscopy
Magnetic resonance imaging and biomedical NMR
Producing an image
Whole body imaging
Diffusion and flow
Chemical shift imaging
Biological uses of imaging - imaging microscopy
Industrial uses of imaging techniques
Biomedical NMR
High-resolution solid-state NMR
Magic angle spinning
Spin-1/2 nuclei with low magnetogyric ratios
I = 1/2 nuclei with high magnetogyric ratios
MAS of quadrupolar nuclei
Some applications
Deuterium, an integral-spin nucleus
Answers to Questions