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Macroscale and Microscale Organic Experiments

ISBN-10: 0538733330

ISBN-13: 9780538733335

Edition: 6th 2011

Authors: Kenneth L. Williamson, Katherine M. Masters

List price: $336.95
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Book details

List price: $336.95
Edition: 6th
Copyright year: 2011
Publisher: Brooks/Cole
Publication date: 5/3/2010
Binding: Hardcover
Pages: 816
Size: 8.75" wide x 11.00" long x 1.25" tall
Weight: 4.070
Language: English

Introduction
Laboratory Safety, Courtesy, and Waste Disposal Techniques
Melting Points and Boiling Points
Recrystallization
Distillation
Steam Distillation, Vacuum Distillation, and Sublimation
Extraction
Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste
Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments
Gas Chromatography: Analysis of Alkene Isomers
Infrared Spectroscopy
Nuclear Magnetic Resonance Spectroscopy
Mass Spectroscopy
Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis
Computational Chemistry Elimination, Substitution, and Addition
The SN2 Reaction: 1-Bromobutane
Nucleophilic Substitution Reactions of Alkyl Halides
Radical Initiated Chlorination of 1-Chlorobutane
Alkenes from Alcohols: Cyclohexene from Cyclohexanol
Bromination and Debromination: Purification of Cholesterol
Dichlorocarbene Oxidation and Reduction
Oxidation: Cyclohexanol to Cyclohexanone
Cyclohexanone to Adipic Acid
The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent
Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol
Catalytic Hydrogenation
Sodium Borohydride Reduction of 2-Methylcyclohexanone: a Problem in Conformational Analysis
Epoxidation of Cholesterol
Aromatic Substitution and Elimination
Nitration of Methyl Benzoate
Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry
Alkylation of Mesitylene
The Friedel-Crafts Reaction: Anthraquinone and Anthracene
Friedel-Crafts Acylation of Ferrocene: Acetylferrocene
Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical
1,2,3,4-Tetraphenylnaphthalene via Benzyne
Triptycene via Benzyne Reactions of Aldehydes and Ketones
Aldehydes and Ketones
Dibenzalacetone by the Aldol Condensation
Grignard Synthesis of Triphenylmethanol and Benzoic Acid
The Wittig and Wittig-Horner Reactions Reactions of Carboxylic Acids, Esters, and Amines
Esterification and Hydrolysis
Acetylsalicylic Acid (Aspirin)
Malonic Ester of a Barbiturate
Amines
The Sandmeyer Reaction: 1-Bromo-4-chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene
Synthesis and Bioessay of Sulfanilamide and Derivatives
Dyes and Dyeing
Martius Yellow
Diels-Alder Reaction
Ferrocene [Bis(cyclopentadienyl)iron]
A Diels-Alder Reaction Puzzle: the Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride
Tetraphenylcyclopentadienone
Hexaphenylbenzene and Dimethyl Tetraphenylphthalate
Derivatives of 1,2-Diphenylethane: a Multistep Synthesis
The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine
Nitric Acid Oxidation
Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline
Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil
The Synthesis of 2,2-Dimethyl-1,5-dioxolane
The Acetonide Derivative of a Vicinal Diol
The 1,4-Addition: Reductive Acetylation of Benzil
Synthesis of an Alkyne from an Alkene
Bromination and Dehydrobromination: Stilbene and Diphenylacetylene
The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid
Multicomponent Reactions: the Aqueous Passerini Reaction
Chemiluminescence: Syntheses of Cyalume and Luminol
Photochemistry: the Synthesis of Benzopinacol Natural Product Chemistry and Biochemistry
Carbohydrates and Sweeteners
Virstatin, a Possible Treatment for Cholera
Biosynthesis of Ethanol and Enzymatic Reactions
The Synthesis of Natural Products: Pseudopellitierene and Camphor
Polymers: Synthesis and Recycling
Searching the Chemical Literature