Modern Organic Synthesis in the Laboratory

Name: Modern Organic Synthesis in the Laboratory
Price: 155.8 USD
Availability: InStock
ISBN: 9780195187984

ISBN-10: 0195187989

ISBN-13: 9780195187984

Edition: 2007

Authors: Jie Jack Li, Chris Limberakis, Derek A. Pflum

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Searching for reaction in organic synthesis has been made much easier in the current age of computer databases. However, the dilemma now is which procedure one selects among the ocean of choices. Especially for novices in the laboratory, it becomes a daunting task to decide what reaction conditions to experiment with first in order to have the best chance of success. This collection intends to serve as an "older and wiser lab-mate" one could have by compiling many of the most commonly used experimental procedures in organic synthesis. With chapters that cover such topics as functional group manipulations, oxidation, reduction, and carbon-carbon bond formation, Modern Organic Synthesis in…

Book details

Copyright year: 2007
Publisher: Oxford University Press, Incorporated
Publication date: 9/10/2007
Binding: Hardcover
Pages: 224
Size: 9.29" wide x 6.30" long x 0.79" tall
Weight: 1.100
Language: English



Foreword


Abbreviations and Acronyms



Fundamental Techniques



Safety!



Useful Preparations



Chromatography



Crystallization



Residual Solvent Peaks in Nuclear Magnetic Resonance



Functional Group Manipulations



Alcohol Oxidation State



Ketone Oxidation State



Acid Oxidation State



Oxidation



Alcohol to Ketone Oxidation State



Alcohol to Acid Oxidation State



Olefin to Diol



Aldehyde to Acid Oxidation State



Heteroatom Oxidations



Reductions



Alcohols to Alkanes



Aldehydes, Amides, and Nitriles to Amines



Carboxylic Acids and Derivatives to Alcohols



Esters and Other Carboxylic Acid Derivatives to Aldehydes



Ketones or Aldehydes to Alcohols



Ketones to Alkanes or Alkenes



Reductive Dehalogenations



Carbon-Carbon Double and Triple Bond Reductions



Heteroatom-Heteroatom Reductions



Carbon-Carbon Bond Formation



Carbon-Carbon Forming Reactions (Single Bonds)



Carbon-Carbon Double Bonds (Olefin Formation)



Reactions that Form Multiple Carbon-Carbon Bonds



Protecting Groups



Alcohols and Phenols



Amines and Anilines



Aldehydes and Ketones


Index