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High-Resolution NMR Techniques in Organic Chemistry

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ISBN-10: 0080427987

ISBN-13: 9780080427980

Edition: 2nd 1999

Authors: Timothy D. W. Claridge

List price: $58.95
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Book details

List price: $58.95
Edition: 2nd
Copyright year: 1999
Publisher: Elsevier Science & Technology Books
Publication date: 12/24/1999
Binding: Hardcover
Pages: 381
Size: 8.50" wide x 12.00" long x 0.75" tall
Weight: 2.530
Language: English

Preface
Acknowledgements
Introduction
The development of high-resolution NMR
Modern NMR and this book
Applying modern NMR techniques
References
Introducing High-resolution NMR
Nuclear spin and resonance
The vector model and pulse excitation
Time and frequency domains
Spin relaxation
Mechanisms for relaxation
References
Practical Aspects of High-resolution NMR
An overview of the NMR spectrometer
Data acquisition and processing
Preparing the sample
Preparing the spectrometer
Spectrometer calibrations
Spectrometer performance tests
References
One-dimensional Techniques
The single-pulse experiment
Spin decoupling methods
Spectrum editing with spin-echoes
Sensitivity enhancement and spectrum editing
Observing quadrupolar nuclei
References
Correlations through the Chemical Bond I: Homonuclear Shift Correlation
Introducing the second dimension
Correlation spectroscopy (COSY)
Practical aspects of 2D NMR
Coherence and coherence transfer
Gradient-selected spectroscopy
Alternative COSY sequences
Total correlation spectroscopy (TOCSY)
Correlating dilute spins: INADEQUATE
References
Correlations through the Chemical Bond II: Heteronuclear Shift Correlation
Introduction
Sensitivity
Heteronuclear single-bond correlation spectroscopy
Heteronuclear multiple-bond correlation spectroscopy
Traditional X-detected correlation spectroscopy
References
Separating Shifts and Couplings: J-resolved Spectroscopy
Introduction
Heteronuclear J-resolved spectroscopy
Homonuclear J-resolved spectroscopy
""Indirect"" homonuclear J-resolved spectroscopy
References
Correlations through Space: The Nuclear Overhauser Effect
Theoretical Aspects
Introduction
Definition of the NOE
Steady-state NOEs
Transient NOEs
Rotating-frame NOEs
Practical Aspects
Measuring steady-state NOEs: NOE difference
Measuring transient NOEs: NOESY
Measuring rotating-frame NOEs: ROESY
Measuring heteronuclear NOEs
Experimental considerations
References
Experimental Methods
Composite pulses
Broadband decoupling and spin-locks
Selective excitation and shaped pulses
Solvent suppression
Recent methods
References
Glossary of Acronyms
Index