Organic Structure Determination Using 2-D NMR Spectroscopy A Problem-Based Approach

Name: Organic Structure Determination Using 2-D NMR Spectroscopy A Problem-Based Approach
Price: 49.42 USD
Availability: InStock
ISBN: 9780123849700

ISBN-10: 0123849705

ISBN-13: 9780123849700

Edition: 2nd 2012

Authors: Jeffrey H. Simpson

List price: $69.95

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Description:

This book contains 30-40 quality 2D NMR data sets following an introductory section describing the methodology employed. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges at the present time are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.. Presents strategies for assigning resonances to known…

Book details

List price: $69.95
Edition: 2nd
Copyright year: 2012
Publisher: Elsevier Science & Technology
Publication date: 2/15/2012
Binding: Paperback
Pages: 540
Size: 7.50" wide x 9.21" long x 1.25" tall
Weight: 2.596
Language: English




Background and Methods



Introduction



Instrumental Considerations



Data Collection, Processing, and Plotting



1H and 13C Chemical Shifts



Symmetry and Topicity



Through-Bond Effects: Spin-Spin (J) Coupling



Through-Space Effects: the Nuclear Overhauser Effect (NOE)



Molecular Dynamics



Strategies for Assigning Molecules



Strategies for Elucidating Unknown Molecular Structures



Problems



Simple Assignment Problems



Complex Assignment Problems



Simple Unknown Problems



Complex Unknown Problems



NMR Resonance Assignment Problems



NMR Unknown Problems