Gas Chromatography and Mass Spectrometry: a Practical Guide

Name: Gas Chromatography and Mass Spectrometry: a Practical Guide
Price: 66.6 USD
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ISBN: 9780123736284

ISBN-10: 0123736285

ISBN-13: 9780123736284

Edition: 2nd 2011

Authors: O. David Sparkman, Zelda Penton, Fulton G. Kitson

List price: $105.00

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Description:

Gas Chromatography and Mass Spectrometry: A Practical Guideis the second edition to the highly successful book of the same name, originally written by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996). Designed as a valuable resource to the GC/MS user, this book provides serves as a one-stop-shop covering updated practical instruction necessary for the successful operation of GC/MS equipment. Includes separation conditions for numerous compound types, instruction on how to interpret mass spectral data, extensive correlations of ion masses and neutral losses with possible structures, together with examples of mass spectra as a means aiding structure determination. Reviews the latest advances…

Book details

List price: $105.00
Edition: 2nd
Copyright year: 2011
Publisher: Elsevier Science & Technology
Publication date: 5/17/2011
Binding: Paperback
Pages: 632
Size: 5.94" wide x 9.00" long x 0.75" tall
Weight: 1.496
Language: English



Preface


Acknowledgments



The Fundamentals of GC/MS



Introduction and History



Gas Chromatography



The GC/MS Interface



Mass Spectrometry Instrumentation



Mass Spectral Data Interpretation



Quantitation with GC/MS



GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types



Acids



Alcohols



Aldehydes



Amides



Amines



Amino Acids



Common Contaminants



Drugs and Their Metabolites



Esters



Ethers



Fluorinated Compounds



Gases



Glycols



Halogenated Compounds (Other Than Fluorinated Compounds)



Hydrocarbons



Isocyanates



Ketones



Nitriles



Nitroaromatics



Nitrogen-Containing Heterocyclic Compounds



Nucleosides (TMS Derivatives)



Pesticides



Phenols



Phosphorus Compounds



Plasticizers and Other Polymer Additives (Including Phthalates)



Prostaglandins (MO-TMS Derivatives)



Solvents and Their Impurities



Steroids



Sugars (Monosaccharides)



Sulfur Compounds



Appendices



Definitions of Terms Related to Gas Chromatography



Definitions of Terms Related to Mass Spectrometry



Atomic Masses and Isotope Abundances and Other Information for the Determination of an Elemental Composition from Isotope Peak Intensity Ratios



X+1 and X+2 Values for Ions Containing Atoms of C and H Based on Isotope Contributions



Isotope Peak Patterns for Ions Containing Atoms of Cl and/or Br



Steps to Follow in the Determination of an Elemental Composition Based on Isotope Peak Intensity Ratios



Derivatization in GC/MS



Points of Comparison of LC/MS vs GC/MS



List of Available EI Mass Spectral Databases



Information Required for Reporting a GC/MS Analysis



Third-Party Software for Use with GC/MS



GC Installation and Maintenance



Troubleshooting Common GC Problems



Maintenance, Operating Tips, and Troubleshooting for Mass Spectrometers



Mixtures for Determining Mass Spectral Resolution



Cross-Index Chart for GC Stationary Phases



Ions for Determining Unknown Structures


Index