Chemical Laboratory Practice

ISBN-10: 3540678158
ISBN-13: 9783540678151
Edition: 3rd 2003 (Revised)
List price: $69.95
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Description: This volume presents in the form of texts, tables, charts and graphs a modern compilation of spectroscopic reference data for IR, UV/Vis, 1H- and 13C-NMR, MS (incl. prototype spectra of almost every important class of organic compounds and spectra  More...

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Book details

List price: $69.95
Edition: 3rd
Copyright year: 2003
Publisher: Springer
Publication date: 3/22/2004
Binding: Hardcover
Pages: 421
Size: 6.00" wide x 9.00" long x 0.75" tall
Weight: 1.496
Language: English

This volume presents in the form of texts, tables, charts and graphs a modern compilation of spectroscopic reference data for IR, UV/Vis, 1H- and 13C-NMR, MS (incl. prototype spectra of almost every important class of organic compounds and spectra of MALDI and FAB matrix materials) and is intended as a short textbook and a hands-on guide for interpreting experimental spectral data and elucidating the chemical structure of the respective compound behind it. The concise texts include special chapters on fragmentation rules in mass spectrometry and on currently used multipulse and 2-D NMR techniques. The book is primarily designed for students to be used during courses and exercises. The use of the book requires only basic knowledge of spectroscopic techniques, but is structured in such a way that it will support practitioners routinely faced with the task of interpreting such spectral information, and it will serve as data reference for specialists in the fields.

Introduction
Scope and Organization
Abbreviations and Symbols
Summary Tables
General Tables
Calculation of the Number of Double Bond Equivalents from the Molecular Formula
Properties of Selected Nuclei
<sup>13</sup>C NMR Spectroscopy
<sup>1</sup>H NMR Spectroscopy
IR Spectroscopy
Mass Spectrometry
Average Masses of Naturally Occurring Elements with Exact Masses and Representative Relative Abundances of Isotopes
Ranges of Natural Isotope Abundances of Selected Elements
Isotope Patterns of Naturally Occurring Elements
Calculation of Isotope Distributions
Isotopic Abundances of Various Combinations of Chlorine, Bromine, Sulfur, and Silicon
Isotope Patterns of Combinations of CI and Br
Indicators of the Presence of Heteratoms
Rules for Determining the Relative Molecular Weight (Mr)
Homologous Mass Series as Indications of Structural Type
Mass Correlation Table
References
UV/Vis Spectroscopy
Combination Tables
Alkanes, Cycloalkanes
Alkenes, Cycloalkenes
Alkynes
Aromatic Hydrocarbons
Heteroaromatic Compounds
Halogen Compounds
Oxygen Compounds
Alcohols and Phenols
Ethers
Nitrogen Compounds
Amines
Nitro Compounds
Thiols and Sulfides
Carbonyl Compounds
Aldehydes
Ketones
Carboxylic Acids
Carboxylic Esters and Lactones
Carboxylic Amides and Lactams
<sup>13</sup>C NMR Spectroscopy
Alkanes
Chemical Shifts
Coupling Constants
References
Alkenes
Chemical Shifts
Coupling Constants
References
Alkynes
Chemical Shifts
Coupling Constants
References
Alicyclics
Chemical Shifts
Coupling Constants
References
Aromatic Hydrocarbons
Chemical Shifts
Coupling Constants
References
Heteroaromatic Compounds
Chemical Shifts
Coupling Constants
Halogen Compounds
Fluoro Compounds
Chloro Compounds
Bromo Compounds
Iodo Compounds
References
Alcohols, Ethers, and Related Compounds
Alcohols
Ethers
Nitrogen Compounds
Amines
Nitro and Nitroso Compounds
Nitrosamines
Imines and Oximes
Hydrazones and Carbodiimides
Nitriles and Isonitriles
Isocyanates, Thiocyanates and Isothiocyanates
References
Sulfur-Containing Functional Groups
Thiols
Sulfides
Disulfides and Sulfonium Salts
Sulfoxides and Sulfones
Sulfonic and Sulfinic Acids and Derivatives
Sulfurous and Sulfuric Acid Derivatives
Sulfur-Containing Carbonyl Derivatives
Carbonyl Compounds
Aldehydes
Ketones
Carboxylic Acids and Carboxylates
Esters and Lactones
Amides and Lactams
Miscellaneous Carbonyl Derivatives
Miscellaneous Compounds
Derivatives of Group IV Elements
Phosphorus Compounds
Miscellaneous Organometallic Compounds
Natural Products
Amino Acids
Carbohydrates
Nucleotides and Nucleosides
Steroids
Spectra of Solvents and Reference Compounds
<sup>13</sup>C NMR Spectra of Common Deuterated Solvents
<sup>13</sup>C NMR Spectra of Secondary Reference Compounds
<sup>13</sup>C NMR Spectrum of a Mixture of Common Nondeuterated Solvents
<sup>1</sup>H NMR Spectroscopy
Alkanes
Chemical Shifts
Coupling Constants
References
Alkenes
Substituted Ethylenes
Dienes
Alkynes
Chemical Shifts and Coupling Constants
Alicyclics
Aromatic Hydrocarbons
Heteroaromatic Compounds
Non-Condensed Heteroaromatic Rings
Condensed Heteroaromatic Rings
Halogen Compounds
Fluoro Compounds
Chloro Compounds
Bromo Compounds
Iodo Compounds
Alcohols, Ethers, and Related Compounds
Alcohols
Ethers
Nitrogen Compounds
Amines
Nitro and Nitroso Compounds
Nitrosamines, Azo, and Azoxy Compounds
Imines, Oximes, Hydrazones, and Azines
Nitriles and Isonitriles
Cyanates, Isocyanates, Thiocyanates, and Isothiocyanates
Sulfur-Containing Functional Groups
Thiols
Sulfides
Disulfides and Sulfonium Salts
Sulfoxides and Sulfones
Sulfonic, Sulfinic, Sulfurous, and Sulfuric Acids and Derivatives
Thiocarboxylate Derivatives
Carbonyl Compounds
Aldehydes
Ketones
Carboxylie Acids and Carboxylates
Esters and Lactones
Amides and Lactams
Miscellaneous Carbonyl Derivatives
Miscellaneous Compounds
Silicon Compounds
Phosphorus Compounds
Miscellaneous Compounds
Natural Products
Amino Acids
Carbohydrates
Nucleotides and Nucleosides
References
Spectra of Solvents and Reference Compounds
<sup>1</sup>H NMR Spectra of Common Deuterated Solvents
<sup>1</sup>H NMR Spectra of Secondary Reference Compounds
1H NMR Spectrum of a Mixture of Common Nondeuterated Solvents
IR Spectroscopy
Alkanes
Alkenes
Monoenes
Allenes
Alkynes
Alicyclics
Aromatic Hydrocarbons
Heteroaromatic Compounds
Halogen Compounds
Fluoro Compounds
Chloro Compounds
Bromo Compounds
Iodo Compounds
Alcohols, Ethers, and Related Compounds
Alcohols and Phenols
Ethers, Acetals, Ketals
Epoxides
Peroxides and Hydroperoxides
Nitrogen Compounds
Amines and Related Compounds
Nitro and Nitroso Compounds
Imines and Oximes
Azo Compounds
Nitriles and Isonitriles
Diazo Compounds
Cyanates and Isocyanates
Thiocyanates and Isothiocyanates
Sulfur-Containing Functional Groups
Thiols and Sulfides
Sulfoxides and Sulfones
Thiocarbonyl Derivatives
Thiocarbonic Acid Derivatives
Carbonyl Compounds
Aldehydes
Ketones
Carboxylie Acids
Esters and Lactones
Amides and Lactames
Acid Anhydrides
Acid Halides
Carbonic Acid Derivatives
Miscellaneous Compounds
Silicon Compounds
Phosphorus Compounds
Boron Compounds
Amino Acids
Solvents, Suspension Media, and Interferences
Infrared Spectra of Common Solvents
Infrared Spectra of Suspension Media
Interferences in Infrared Spectra
Mass Spectrometry
Alkanes
Unbranched Alkanes
Branched Alkanes
References
Alkenes
Unbranched Alkenes
Branched Alkenes
Polyenes and Polyynes
References
Alkynes
Aliphatic Alkynes
References
Alicyclic Hydrocarbons
Cyclopropanes
Saturated Monocyclic Alicyclics
Polycyclic Alicyclics
Cyclohexenes
References
Aromatic Hydrocarbones
Aromatic Hydrocarbons
Alkylsubstituted Aromatic Hydrocarbons
References
Heteroaromatic Compounds
General Characteristics
Furans
Thiophenes
Pyrroles

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