Introduction to Mass Spectrometry Instrumentation, Applications and Strategies for Data Interpretation

ISBN-10: 0470516348
ISBN-13: 9780470516348
Edition: 4th 2007
List price: $140.00 Buy it from $74.98
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Description: Completely revised and updated, this text provides an easy-to-read guide to the concept of mass spectrometry and demonstrates its potential and limitations. Written by internationally recognised experts and utilising "real life" examples of analyses  More...

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Book details

List price: $140.00
Edition: 4th
Copyright year: 2007
Publisher: John Wiley & Sons, Incorporated
Publication date: 11/12/2007
Binding: Hardcover
Pages: 862
Size: 8.00" wide x 9.75" long x 1.75" tall
Weight: 4.202
Language: English

Completely revised and updated, this text provides an easy-to-read guide to the concept of mass spectrometry and demonstrates its potential and limitations. Written by internationally recognised experts and utilising "real life" examples of analyses and applications, the book presents real cases of qualitative and quantitative applications of mass spectrometry. Unlike other mass spectrometry texts, this comprehensive reference provides systematic descriptions of the various types of mass analysers and ionisation, along with corresponding strategies for interpretation of data. The book concludes with a comprehensive 3000 references.This multi-disciplined text covers the fundamentals as well as recent advance in this topic, providing need-to-know information for researchers in many disciplines including pharmaceutical, environmental and biomedical analysis who are utilizing mass spectrometry

Introduction
What is Mass Spectrometry
History
Applications
The Data of Mass Spectrometry and Its Presentation
Spectra
Total Ion Current
Mass Chromatograms and Profiles
Definition of Terms
Mass-To-Charge Ratio (m/z)
Multiple-Charge Ions
Ions Representing an Intact Molecule
Resolution/Resolving Power
Intensity vs Abundance
The Mass Spectrometer
Introduction
Ion Guides
Types of m/z Analyzers
Time-Of-Flight
Linear.1) Resolving Power of the Linear TOF Instrument.2) Time-Lag Focusing.3) Beam Deflection
Reflectron
Orthogonal Acceleration
Ion Detection in the TOF Analyzer.1) Time Slice Detection.2) Time Array Detection.3) TAD with Transient Recorders.4) TAD with an Integrating Transient Recorder.5) Hadamard Transform TOF MS
Quadrupole Ion Traps
3D Quadrupole Ion Traps
Linear Quadrupole Ion Traps
Orbitrap
Historical Aspects
Operating Principles
Transmission Quadrupoles
QMF Equations of Motion
The Stability Diagram
Characteristics of Output
Spectral Skewing
Performance Limitations
Sector instruments
Single-focusing Instruments.1) Operating Principles.2) Performance Limitations
Double-Focusing Instruments
FTICR-MS
Hardware Configuration
Operational Considerations
Representative Applications
Calibration of the m/z Scale
Electron Ionizaton (GC/MS)
Chemical Ionization (GC/MS)
Electrospray and Other Atmospheric Pressure Ionization Techniques
Ion Detection
General Considerations
Types of Detectors
Faraday Cup
Electron Multiplier.1) Discrete-Dynode Version.2) Continuous-Dynode Version
Negative-Ion Detection
Post-Acceleration Detection and Detection of High-Mass Ions
Channel Electron Multiplier Array (CEMA)
Electro-Optical Ion Detection
The Daly Detector
Cryogenic Detectors
Vacuum Systems
Introduction
Definitions
Pressure Gauges
Thermal-Conductivity Gauges
Ionization Gauges
Types of Pumps
Mechanical Pumps (Low Vacuum).1) Rotary Vane.2) Scroll.3) Diaphram
High Vacuum.1) Turbomolecular Pumps.2) Diffusion Pumps.3) Sputter-Ion Pumps.4) Cryogenic Pumps
Mass Spectrometry/Mass Spectrometry
Introduction
Concept and Definitions
Nomenclature
Ion Dissociation
Metastable Ions
Instrumentation for MS/MS
MS/MS in Space
Tandem MS/MS.1) Triple-Quadrupole Mass Spectrometer.2) BEqQ Hybrid Instrument
Double-Focusing Instruments
MS/MS in Time
Specialized Techniques and Applications
In-Source CAD
CAD in Conjunction with Soft Ionization
Selected Reaction Monitoring
Precursor-Ion Scan
Neutral Loss (Common Loss) Scan
Ion/Molecule Reactions
Identification of Unknowns from CAD Data
Accurate Mass Measurements
Library Search Utilities
Other Databases
Substructure Information
Use of MS Interpreter
Inlet Systems
Introduction
Batch Inlets
Heated Reservoir Inlet
Direct Inlet Probe (DIP)
The Chromatoprobe
Direct Exposure Probe (Desorption Chemical Ionization [DCI])
Pyrolysis
Continuous Inlets

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