Organic Structure Analysis

ISBN-10: 0195336046

ISBN-13: 9780195336047

Edition: 2nd 2010

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Description:

The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis,organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods.
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Book details

List price: $199.95
Edition: 2nd
Copyright year: 2010
Publisher: Oxford University Press, Incorporated
Publication date: 10/29/2009
Binding: Hardcover
Pages: 656
Size: 8.75" wide x 11.25" long x 1.00" tall
Weight: 4.048
Language: English

Preface
Using Spectroscopic Data In Organic Structure Analysis
A Glimpse of the Methods in Common Use
Characteristics of the Methods in Common Use
Steps in Establishing a Molecular Structure
Molecular Formula (MF) and Unsaturation Number (UN)
Substructures, Working Structures, and Final Structures
Limitations of Spectroscopic Data in Structure Analysis
Introduction To Nuclear Magnetic Resonance
A Glimpse of the NMR Phenomenon
Commonly Studied Nuclei
Obtaining an NMR Spectrum
Magnetic Shielding
Relaxation Effects
Effect of Relaxation and NOE on Peak Intensities
Electric Quadrupole Effects
Measurement and Presentation of Data
Sample Preparation and Sample Size
Common Impurities in NMR Spectra
Other Useful Nuclei
Interpretation And Use Of Proton And Carbon Chemical Shifts
A Glimpse of Chemical Shifts and Peak Areas
Terms and Conventions
Factors That Determine Chemical Shifts
Chemical Shift Positions of 1H/13C Attached to Common Functional Groups
Chemical Shift Equivalence
Characteristic Chemical Shifts for Different Protons and Carbons
Using Databases to Estimate 13C NMR Chemical Shifts
Making Configurational Assignments Based on Chemical Shifts: Case Examples
Interpretation And Use Of Proton And Carbon Coupling Constants
A Glimpse of Coupling Constants
First-Order Spectra and the n + 1 Rule
Terms and Conventions
Common Coupled Spin Systems
Magnetic Nonequivalence
Using Coupling Constants to Understand the Appearance of Spectra and Make Assignments
Coupling Constant Values for Different Carbon and Proton Types
Using Coupling Constants to Make Configurational Assignments
Ways to Simplify or Eliminate Coupling Effects
The Nuclear Overhauser effect
Additional Ways to Obtain J Values
Multiple-Pulse And Multidimensional Nmr Techniques
A Glimpse of Multiple-Pulse NMR Methods
Elements of Multiple-Pulse NMR
One-Dimensional NMR Techniques
Two-Dimensional NMR Techniques
Using Two-Dimensional NMR in Assigning Spectra
Using Two-Dimensional NMR Data to Determine an Unknown Structure
Strategies for Using 2D NMR in Structure Determination
Use of NOESY and ROESY to Determine Relative Stereochemistry and Conformations
Specialized Pulse Sequences
Configurational Analysis Based on Coupling Constants: Experimental Measurement of 2.3 JCH
Computer-Assisted Structure Elucidation
Future Prospects in Multidimensional NMR
Mass Spectrometry: Core Techniques And Ionization Processes
A Glimpse of Mass Spectrometry
Measurement, Presentation of Data, and Nomenclature
Isotopes, Atomic Composition, Molecular Formulas, and Ionic Mass: Low and High Resolution and Measurements
Different Ionization Techniques in Mass Spectrometry
Different Techniques for Analyzing Ions in Mass Spectrometry
Detectors in Mass Spectrometry
Hyphenated Mass Spectrometry
Tandem Mass Spectrometry
Future Prospects
Mass Spectrometry Analysis Of Small And Large Molecules
A Glimpse of Molecular Ions Revisited
Small-Molecule Mass Spectral Analysis
Large-Molecule Mass Spectrometry
Future Prospects
Fragmentation Processes In Electron Ionization Mass Spectrometry
A Glimpse of Fragmentation in Mass Spectrometry
Interpreting a Low Resolution Electron Ionization Mass Spectrum
Fragmentation Processes
Identification of Functionality from Fragmentation Processes
Schematic Approach for the Interpretation of an EIMS
Infrared Spectroscopy
A Glimpse of Infrared Spectroscopy
Measurement and Presentation of Data
The Fundamentals
Identifying Functional Groups
Interpreted Infrared Spectra
Use of Infrared Databases
Optical And Chiroptical Techniques: Ultraviolet Spectroscopy
A Glimpse of Ultraviolet Spectroscopy
Measurement and Presentation of Data
The Fundamentals for Interpreting Spectra
Identifying Functional Groups
Theoretical Simulations of UV Spectra
The Behavior of Chiral Chromophores ORD/CD
The Exciton Chirality Method
Other Ways to Examine Chiral Chromophores
Strategies Of Determining Structure And Stereochemistry: Spectroscopic Data Translated Into Structures
A Glimpse of the Combined Use of Spectroscopic Data
The Strategies of Determining Structure and Stereochemistry
Dereplication Strategies
Worked Examples of Deriving Structures from Spectroscopic Data
Problems In Organic Structure Analysis
A Glimpse of the Scope of the 51 Unknowns
Using the Spectra, Accompanying Information, and Other Resources
Appendices
Collections of Spectra or Data Tables
Shape of MS Clusters
CAS Registry Numbers for Unknowns
Glossary and Abbreviations
Index
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