Operational Organic Chemistry A Problem-Solving Approach to the Laboratory Course

ISBN-10: 0138419175
ISBN-13: 9780138419172
Edition: 3rd 1999 (Revised)
Authors: John W. Lehman
List price: $133.20
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Description: This experimental chemistry text prepares students to perform fundamental operations in the lab, and to apply these to new situations. A new methodology section focuses on developing a hypothesis, designing an experiment and evaluating results.

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Book details

List price: $133.20
Edition: 3rd
Copyright year: 1999
Publisher: Prentice Hall PTR
Publication date: 8/12/1998
Binding: Hardcover
Pages: 808
Size: 8.25" wide x 10.50" long x 1.25" tall
Weight: 3.630
Language: English

This experimental chemistry text prepares students to perform fundamental operations in the lab, and to apply these to new situations. A new methodology section focuses on developing a hypothesis, designing an experiment and evaluating results.

To the Instructor
Introduction
Laboratory Safety
Mastering the Operations
Learning Basic Operations
The Effect of pH on a Food Preservative
Extraction and Evaporation
Separating the Components of Panacetin
Recrystallization and Melting Point Measurement
Identifying a Constituent of Panacetin
Heating under Reflux
Synthesis of Salicylic Acid from Wintergreen Oil
Simple Distillation, Gas Chromatography
Preparation of Synthetic Banana Oil
Fractional Distillation
Separation of Petroleum Hydrocarbons
Addition, Mixing, Sublimation
Preparation of Camphor
Boiling Point, Refractive Index
Identification of a Petroleum Hydrocarbon
Column Chromatography, UV-VIS Spectrometry
Isolation and Isomerization of Lycopene from Tomato Paste
Steam Distillation, Infrared Spectrometry
Isolation and Identification of the Major Constituent of Clove Oil
Thin-Layer Chromatography, NMR Spectrometry
Identification of Unknown Ketones
Vacuum Distillation, Optical Rotation
Optical Activity of ...a-Pinene
Correlated Laboratory Experiments
Investigation of a Chemical Bond by Infrared Spectrometry
Properties of Common Functional Groups
Thin-Layer Chromatographic Analysis of Drug Components
Separation of an Alkane Clathrate
Isomers and Isomerization Reactions
Structures and Properties of Stereoisomers
Bridgehead Reactivity in an SN1 Solvolysis Reaction
Reaction of Iodoethane with Sodium Saccharin, an Ambident Nucleophile
Dehydration of Methylcyclohexanols
Synthesis of 7,7-Dichloronorcarane Using a Phase-Transfer Catalyst
Stereochemistry of the Addition of Bromine to trans-Cinnamic Acid
Hydration of a Difunctional Alkyne
Preparation of Bromotriphenylmethane and the Trityl Free Radical
Chain-Growth Polymerization of Styrene and Methyl Methacrylate
Synthesis of Ethanol by Fermentation
The Reaction of Butanols with Hydrobromic Acid
Borohydride Reduction of Vanillin
Multistep Synthesis of Cyclopentanol from Cyclohexanol
Synthesis of Triphenylmethanol and the Trityl Carbocation
Identification of a Conjugated Diene from Eucalyptus Oil
Spectral Identification of Terpenoids
Synthesis and Spectral Analysis of Aspirin
Preparation of Nonbenzenoid Aromatic Compounds
Mechanism of the Nitration of Arenes by Nitronium Fluoborate
Friedel-Crafts Acylation of Anisole
Structure of a Natural Product in Anise Oil
Identification of an Oxygen-Containing Organic Compound
Wittig Synthesis of 1,4-Diphenyl-1,3-Butadiene
Effect of Reaction Conditions on the Condensation of Furfural with Cyclopentanone
Haloform Oxidation of 4'-Methoxyacetophenone
Electronic Effect of a para-Iodo Substituent
Synthesis and Identification of an Unknown Carboxylic Acid
Preparation of the Insect Repellent N, N- Diethyl-m-Toluamide
Synthesis of 2-Acetylcyclohexanone by the Stork Enamine Reaction
Synthesis of Dimedone and Measurement of Its Tautomeric Equilibrium Constant
Preparation of Para Red and Related Azo Dyes
Reaction of Phthalimide with Sodium Hypochlorite
Identification of an Unknown Amine
Preparation and Mass Spectrum of 2-Phenylindole
Nucleophilic Strength an

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