Multiscale Operational Organic Chemistry A Problem-Solving Approach to the Laboratory Course

ISBN-10: 0130154954

ISBN-13: 9780130154958

Edition: 2002

Authors: John W. Lehman
List price: $120.40
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Description: For the undergraduate organic chemistry course. This practical laboratory text provides a thorough introduction to the core operations in the organic lab in addition to both microscale and traditional-scale experiments. Its unique problem-solving approach encourages students to think in the laboratory by solving a scientific problem in the process of carrying out each experiment.

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Book details

List price: $120.40
Copyright year: 2002
Publisher: Prentice Hall PTR
Publication date: 8/20/2001
Binding: Hardcover
Pages: 864
Size: 8.00" wide x 10.00" long x 1.50" tall
Weight: 3.850
Language: English

Preface
Introduction
Mastering the Operations
Learning Basic Operations
The Effect of pH on a Food Preservative
Extraction and Evaporation
Separating the Components of Panacetin
Recrystallization and Melting-Point Measurement
Identifying a Constituent of Panacetin
Heating under Reflux
Synthesis of Salicylic Acid from Wintergreen Oil
Simple Distillation, Gas Chromatography
Preparation of Synthetic Banana Oil
Fractional Distillation
Separation of Petroleum Hydrocarbons
Addition, Mixing, Sublimation
Preparation of Camphor
Boiling Point, Refractive Index
Identification of a Petroleum Hydrocarbon
Column Chromatography, UV-VIS Spectrometry
Isolation and Isomerization of Lycopene from Tomato Paste
Steam Distillation, Infrared Spectrometry
Isolation and Identification of the Major Constituent of Clove Oil
Thin-Layer Chromatography, NMR Spectrometry
Identification of Unknown Ketones
Vacuum Distillation, Optical Rotation
Optical Activity of a-Pinene
Correlated Laboratory Experiments
Investigation of a Chemical Bond by Infrared Spectrometry
Properties of Common Functional Groups
Thin-Layer Chromatographic Analysis of Drug Components
Separation of an Alkane Clathrate
Isomers and Isomerization Reactions
Structures and Properties of Stereoisomers
Bridgehead Reactivity in an Sn1 Solvolysis Reaction
Reaction of Iodoetane with Saccharin, an Ambident Nucleophile
Dehydration of Methylcyclohexanols
Synthesis of 7,7-Dichloronorcarane Using a Phase-Transfer Catalyst
Stereochemistry of the Addition of Bromine to trans-Cinnamic Acid
Preparation of Bromotriphenylmethane and the Trityl Free Radical
Chain-Growth Polymerization of Styrene and Methyl Methacrylate
Synthesis of Ethanol by Fermentation
Reaction of Butanols with Hydrobromic Acid
Borohydride Reduction of Vanillin to Vanillyl Alcohol
Synthesis of Triphenylmethanol and the Trityl Carbocation
Identification of a Conjugated Diene from Eucalyptus Oil
Spectral Identification of Terpenoids
Synthesis and Spectral Analysis of Aspirin
Preparation of Nonbenzenoid Aromatic Compounds
Mechanism of the Nitration of Arenes by Nitronium Fluoborate
Friedel-Crafts Acylation of Anisole
Structure of a Natural Product in Anise Oil
Identification of an Oxygen-Containing Organic Compound
Wittig Synthesis of 1,4-Diphenyl-1,3-Butadiene
Effect of Reaction Conditions on the Condensation of Furfural with Cyclopentanone
Haloform Oxidation of 4'-Methoxyacetophenone
Electronic Effect of a para-Iodo Substituent
Synthesis and Identification of an Unknown Carboxylic Acid
Preparation of the Insect Repellent N,N-Diethyl-meta-Toluamide
Synthesis of Dimedone and Measurement of its Tautomeric Equilibrium Constant
Preparation of Para Red and Related Azo Dyes
Reaction of Phthalimide with Sodium Hypochlorite
Identification of an Unknown Amine
Preparation and Mass Spectrum of 2-Phenylindole
Nucleophilic Strength and Reactivity in SnAr Reactions
Structure of an Unknown D-Hexose
Fatty Acid Content of Commercial Cooking Oils
Structure of an Unknown Dipeptide
Multistep Synthesis of Benzilic Acid from Be
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