Gas Chromatography and Mass Spectrometry A Practical Guide

ISBN-10: 0123736285

ISBN-13: 9780123736284

Edition: 2nd 2008

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Description: Gas Chromatography and Mass Spectrometry: A Practical Guideis the second edition to the highly successful book of the same name, originally written by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996). Designed as a valuable resource to the GC/MS user, this book provides serves as a one-stop-shop covering updated practical instruction necessary for the successful operation of GC/MS equipment. Includes separation conditions for numerous compound types, instruction on how to interpret mass spectral data, extensive correlations of ion masses and neutral losses with possible structures, together with examples of mass spectra as a means aiding structure determination. Reviews the latest advances in instrumentation, ionization methods, and quantitation; updated tips on the operation of mass spectrometers and derivatization procedures; troubleshooting techniques and a variety of other information useful for the practising GC/MS user. * Serves as a one-stop-shop covering updated practical instruction necessary for the successful operation of GC/MS equipment * Reviews the latest advances in instrumentation, ionization methods, and quantitation * Includes troubleshooting techniques and a variety of other information useful for the practising GC/MS user

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Book details

List price: $105.00
Edition: 2nd
Copyright year: 2008
Publisher: Elsevier Science & Technology Books
Publication date: 3/30/2011
Binding: Paperback
Pages: 632
Size: 6.00" wide x 8.75" long x 0.75" tall
Weight: 2.178

Preface
Acknowledgments
The Fundamentals of GC/MS
Introduction and History
Gas Chromatography
The GC/MS Interface
Mass Spectrometry Instrumentation
Mass Spectral Data Interpretation
Quantitation with GC/MS
GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types
Acids
Alcohols
Aldehydes
Amides
Amines
Amino Acids
Common Contaminants
Drugs and Their Metabolites
Esters
Ethers
Fluorinated Compounds
Gases
Glycols
Halogenated Compounds (Other Than Fluorinated Compounds)
Hydrocarbons
Isocyanates
Ketones
Nitriles
Nitroaromatics
Nitrogen-Containing Heterocyclic Compounds
Nucleosides (TMS Derivatives)
Pesticides
Phenols
Phosphorus Compounds
Plasticizers and Other Polymer Additives (Including Phthalates)
Prostaglandins (MO-TMS Derivatives)
Solvents and Their Impurities
Steroids
Sugars (Monosaccharides)
Sulfur Compounds
Appendices
Definitions of Terms Related to Gas Chromatography
Definitions of Terms Related to Mass Spectrometry
Atomic Masses and Isotope Abundances and Other Information for the Determination of an Elemental Composition from Isotope Peak Intensity Ratios
X+1 and X+2 Values for Ions Containing Atoms of C and H Based on Isotope Contributions
Isotope Peak Patterns for Ions Containing Atoms of Cl and/or Br
Steps to Follow in the Determination of an Elemental Composition Based on Isotope Peak Intensity Ratios
Derivatization in GC/MS
Points of Comparison of LC/MS vs GC/MS
List of Available EI Mass Spectral Databases
Information Required for Reporting a GC/MS Analysis
Third-Party Software for Use with GC/MS
GC Installation and Maintenance
Troubleshooting Common GC Problems
Maintenance, Operating Tips, and Troubleshooting for Mass Spectrometers
Mixtures for Determining Mass Spectral Resolution
Cross-Index Chart for GC Stationary Phases
Ions for Determining Unknown Structures
Index
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