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Preface | |
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The calorimeter as an object with a heat source | |
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The Fourier law and the Fourier-Kirchhoff equation | |
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Heat transfer. Conduction, convection and radiation | |
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General integral of the Fourier equation. Cooling and heating processes | |
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Heat balance equation of a simple body. The Newton law of cooling | |
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The heat balance equations for a rod and sphere | |
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General heat balance equation of a calorimetric system | |
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Calorimeters as dynamic objects | |
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Types of dynamic objects | |
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Laplace transformation | |
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Dynamic time-resolved characteristics | |
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Pulse response | |
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Frequential characteristics | |
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Calculations of spectrum transmittance | |
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Methods of determination of dynamic parameters | |
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Determination of time constant | |
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Least squares method | |
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Modulating functions method | |
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Rational function method of transmittance approximation | |
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Determination of parameters of spectrum transmittance | |
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Classification of calorimeters. Methods of determination of heat effects | |
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Classification of calorimeters | |
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Methods of determination of heat effects | |
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General description of methods of determination of heat effects | |
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Comparative method of measurements | |
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Adiabatic method and its application in adiabatic and scanning adiabatic calorimetry | |
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Multidomains method | |
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Finite elements method | |
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Dynamic method | |
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Flux method | |
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Modulating method | |
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Steady-state method | |
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Method of corrected temperature rise | |
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Numerical and analog methods of determination of thermokinetics | |
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Harmonic analysis method | |
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Method of dynamic optimization | |
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Thermal curve interpretation method | |
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Method of state variables | |
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Method of transmittance decomposition | |
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Inverse filter method | |
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Evaluation of methods of determination of total heat effects and thermokinetics | |
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Linearity and principle of superposition | |
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Dynamic properties of calorimeters | |
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Equations of dynamics | |
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Dynamic properties of two and three-domain calorimeters with cascading structure | |
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Equations of dynamics. System of two domains in series | |
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Equations of dynamics. Three domains in series | |
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Applications of equations of dynamics of cascading systems | |
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Dynamic properties of calorimeters with concentric configuration | |
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Dependence of dynamic properties of two-domain calorimeter with concentric configuration on location of heat sources and temperature sensors | |
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Dependence between temperature and heat effect as a function of location of heat source and temperature sensor | |
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Apparent heat capacity | |
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Energy equivalent of calorimetric system | |
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Final remarks | |
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References | |