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Mass Spectrometry | |
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Introduction | |
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Instrumentation | |
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Ionization Methods | |
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Mass Analyzers | |
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Interpretation of El Mass Spectra | |
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Mass Spectra of Some Chemical Classes | |
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Infrared Spectrometry | |
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Introduction | |
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Theory | |
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Instrumentation | |
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Sample Handling | |
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Interpretations of Spectra | |
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Characteristic Group Absorption of Organic Molecules | |
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Proton Magnetic Resonance Spectrometry | |
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Introduction | |
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Theory | |
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Instrumentation and Sample Handling | |
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Chemical Shift | |
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Spin Coupling, Multiplets, Spin Systems | |
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Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons | |
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Coupling of Protons to Other Important Nuclei ( 19 F, E, 31 P, 29 Si, and 13 C | |
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Chemical Shift Equivalence | |
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Magnetic Equivalence (Spin-Coupling Equivalence) | |
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AMX, ABX, and ABC Rigid Systems with Three Coupling Constants | |
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Confirmationally Mobile, Open-Chain Systems. Virtual Coupling | |
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Chirality | |
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Vicinal and Geminal Coupling | |
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Low-Range Coupling | |
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Selective Spin Decoupling. Double Resonance | |
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Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space | |
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Carbon-13 NMR Spectrometry | |
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Introduction | |
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Theory | |
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Interpretation of a Simple 13 C Spectrum: Diethyl Phthalate | |
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Quantitative 13 C Analysis | |
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Chemical Shift Equivalence | |
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DEPT | |
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Chemical Classes and Chemical Shifts | |
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Correlation NMR Spectrometry; 2-D NMR | |
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Introduction | |
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Theory | |
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Correlation Spectrometry | |
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Ipsenol: 1 H- 1 H COSY | |
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Caryophyllene Oxide | |
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13 C- 13 C Correlations: Inadequate | |
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Lactose | |
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Relayed Coherence Transfer: TOCSY | |
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HMQC - TOCSY | |
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ROESY | |
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VGSE | |
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Gradient Field NMR | |
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NMR Spectrometry of Other Important Spin 1/2 Nuclei | |
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Introduction | |
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15 N Nuclear Magnetic Resonance | |
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19 F Nuclear Magnetic Resonance | |
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29 Si Nuclear Magnetic Resonance | |
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31 P Nuclear Magnetic Resonance | |
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Conclusion | |
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Solved Problems | |
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Introduction | |
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Assigned Problems | |
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Introduction | |