Basic Gas Chromatography

ISBN-10: 0470439548

ISBN-13: 9780470439548

Edition: 2nd 2009

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Description:

This is the second, updated edition of the very successful first edition by these co-authors. It contains new up-to-date information on the field and has been expanded by several chapters, including one on multidimensional gas chromatography and another on sampling methods, as well as special injection techniques and fast gas chromatography. The new edition would still have the same goals as the first, though. As stated in the preface of the first edition: "We have attempted to write a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject."
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Book details

List price: $47.95
Edition: 2nd
Copyright year: 2009
Publisher: John Wiley & Sons, Limited
Publication date: 7/17/2009
Binding: Hardcover
Pages: 256
Size: 6.50" wide x 9.50" long x 1.00" tall
Weight: 1.320
Language: English

#60;b#62;Harold M. Mcnair, PhD#60;/b#62;, known internationally as a leading researcher and educator in the field of chromatography, is currently Professor Emeritus of Chemistry at Virginia Tech.#60;p#62;#60;b#62;James M. Miller, PhD#60;/b#62;, is Professor Emeritus of Chemistry at Drew University, where he taught for thirty-six years. He is also the author of #60;i#62;Chromatography: Concepts and Contrasts#60;/i#62; (Wiley).

Preface to the Second Edition
Preface
Acknowledgments
Introduction
A Brief History
Definitions
Overview: Advantages and Disadvantages
Instrumentation
References
Instrument Overview
Carrier Gas
Flow Control and Measurement
Sample Inlets and Sampling Devices
Columns
Temperature Zones
Detectors
Data Systems
References
Basic Concepts and Terms
Definitions, Terms, and Symbols
The Rate Theory
A Redefinition of H
The Achievement of Separation
References
Stationary Phases
Selecting a Column
Classification of Stationary Phases for GLC
Liquid Stationary Phases (GLC)
Solid Stationary Phases (GSC)
References
Packed Columns and Inlets
Solid Supports
Liquid Stationary Phases
Solid Stationary Phases (GSC)
Gas Analysis
Analysis of Other Inorganics
Inlets for Liquid Samples and Solutions
Special Columns
Upgrading for Capillary Columns
References
Capillary Columns and Inlets
Types of OT Columns
OT Column Tubing
Advantages of OT Columns
Column Selection
Capillary Inlet Systems
Miscellaneous Topics
References
Detectors
Classification of Detectors
Detector Characteristics
Flame Ionization Detector (FID)
Thermal Conductivity Detector (TCD)
Electron Capture Detector (ECD)
Other Detectors
References
Qualitative and Quantitative Analysis
Qualitative Analysis
Quantitative Analysis
References
Programmed Temperature
Temperature Effects
Advantages and Disadvantages of PTGC
Requirements of PTGC
Theory of PTGC
Special Topics
References
Gas Chromatography-Mass Spectrometry (GC-MS)
Instrumentation
History
Limitations of GC-MS Systems
Data Analysis
References
Multidimensional Gas Chromatography
Overview
Fundamental Principles of Multidimensional Chromatography
GC�GC with Heart Cutting
Comprehensive GC�GC
LC�GC with Heart Cutting
Comprehensive LC�GC
Summary
References
Sampling Methods
Overview
Liquid-Liquid Extraction (LLE)
Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE)
Liquid-Solid Extraction: Solid-Phase Extraction (SPE)
Liquid- or Solid-Vapor Extraction: Headspace Extraction
Solid-Phase Micro-extraction (SPME)
Additional Techniques and Summary
References
Special Topics
Fast GC
Chiral Analysis by GC
GC Analysis of Nonvolatile Compounds
References
Troubleshooting GC Systems
Symbols and Acronyms
Guidelines for Selecting Capillary Columns
GC: How to Avoid Problems
Calculation of Split Ratio for Split Injection on OT Columns
Operating Conditions for Capillary Columns
OV Liquid Phases Physical Property Data
Some Compressibility Correction Factors (J)
Some Internet Websites for Gas Chromatographers
Other Books on Gas Chromatography
Index of Applications
Index
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