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Experimental Organic Chemistry A Small Scale Approach

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ISBN-10: 002427691X

ISBN-13: 9780024276919

Edition: 2nd 1995 (Revised)

Authors: Charles F. Wilcox, Mary F. Wilcox

List price: $206.65
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Description:

Takes a small scale approach to experimentation, keeping costs of material and their disposal down by a factor of five coompared to standard scale, while retaining most standard scale equipment and requiring no special glassware. The previous edition ISBN is: 0-02-427620-0.
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Book details

List price: $206.65
Edition: 2nd
Copyright year: 1995
Publisher: Prentice Hall PTR
Publication date: 10/26/1994
Binding: Paperback
Pages: 560
Size: 7.75" wide x 9.75" long x 1.00" tall
Weight: 2.530
Language: English

I. INTRODUCTION. 1. Safety in the Laboratory. 2. General Remarks. 3. Basic Laboratory Operations. 4. Accessory Operations. II. SEPARATION AND PURIFICATION OF ORGANIC COMPOUNDS. 5. Simple and Fractional Distillation. 6. Vacuum Distillation. 7. Steam Distillation. 8. Melting Points, Crystallization, and Sublimation. 9. Extraction with Solvents. 10. Chromatography. III. IDENTIFICATION OF ORGANIC COMPOUNDS. 11. Identification by Chemical Methods. 12. Mass Spectrometry. 13. Infrared Spectroscopy. 14. Visible and Invisible Ultraviolet Spectroscopy. 15. Nuclear Magnetic Resonance. IV. PREPARATION AND REACTIONS OF TYPICAL ORGANIC COMPOUNDS. 16.…