| |
| |
Acronyms | |
| |
| |
Preface | |
| |
| |
| |
Microscopy with light and electrons | |
| |
| |
| |
Introduction | |
| |
| |
| |
Methods of image formation | |
| |
| |
| |
Pixels | |
| |
| |
| |
The light-optical microscope | |
| |
| |
| |
Magnification | |
| |
| |
| |
Resolution | |
| |
| |
| |
Depth of field and depth of focus | |
| |
| |
| |
Aberrations in optical systems | |
| |
| |
| |
Electrons versus light | |
| |
| |
| |
Questions | |
| |
| |
| |
Electrons and their interaction with the specimen | |
| |
| |
| |
Introduction | |
| |
| |
| |
Electrons | |
| |
| |
| |
Generating a beam of electrons | |
| |
| |
| |
Deflection of electrons--magnetic lenses | |
| |
| |
| |
The scattering of electrons by atoms | |
| |
| |
| |
Elastic scattering | |
| |
| |
| |
Inelastic scattering | |
| |
| |
| |
Secondary effects | |
| |
| |
| |
The family of electron microscopes | |
| |
| |
| |
Questions | |
| |
| |
| |
Electron diffraction | |
| |
| |
| |
The geometry of electron diffraction | |
| |
| |
| |
Diffraction spot patterns | |
| |
| |
| |
Use of the reciprocal lattice in diffraction analysis | |
| |
| |
| |
Other types of diffraction pattern | |
| |
| |
| |
Questions | |
| |
| |
| |
The transmission electron microscope | |
| |
| |
| |
The instrument | |
| |
| |
| |
Contrast mechanisms | |
| |
| |
| |
High voltage electron microscopy (HVEM) | |
| |
| |
| |
Scanning transmission electron microscopy (STEM) | |
| |
| |
| |
Preparation of specimens for TEM | |
| |
| |
| |
Questions | |
| |
| |
| |
The scanning electron microscope | |
| |
| |
| |
How it works | |
| |
| |
| |
Obtaining a signal in the SEM | |
| |
| |
| |
The optics of the SEM | |
| |
| |
| |
The performance of the SEM | |
| |
| |
| |
The ultimate resolution of the SEM | |
| |
| |
| |
Topographic images | |
| |
| |
| |
Compositional images | |
| |
| |
| |
Crystallographic information from the SEM | |
| |
| |
| |
The use of other signals in the SEM | |
| |
| |
| |
Image acquisition, processing and storage | |
| |
| |
| |
The preparation of specimens for examination in the SEM | |
| |
| |
| |
Low voltage microscopy | |
| |
| |
| |
Environmental scanning electron microscopy (ESEM) | |
| |
| |
| |
Questions | |
| |
| |
| |
Chemical analysis in the electron microscope | |
| |
| |
| |
The generation of X-rays within a specimen | |
| |
| |
| |
Detection and counting of X-rays | |
| |
| |
| |
X-ray analysis of bulk specimens | |
| |
| |
| |
X-ray analysis of thin specimens in the TEM | |
| |
| |
| |
Quantitative analysis in an electron microscope | |
| |
| |
| |
Electron energy loss spectroscopy (EELS) | |
| |
| |
| |
A brief comparison of techniques | |
| |
| |
| |
Questions | |
| |
| |
| |
Electron microscopy and other techniques | |
| |
| |
| |
Complementary imaging techniques | |
| |
| |
| |
Complementary analysis techniques--alternative analysis systems | |
| |
| |
| |
Complementary diffraction techniques | |
| |
| |
| |
Summary | |
| |
| |
| |
Questions | |
| |
| |
Further reading | |
| |
| |
Answers | |
| |
| |
Index | |