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Experimental Organic Chemistry A Miniscale and Microscale Approach

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ISBN-10: 049501334X

ISBN-13: 9780495013341

Edition: 4th 2006 (Revised)

Authors: John C. Gilbert, Stephen F. Martin

List price: $373.95
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Description:

This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required…    
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Book details

List price: $373.95
Edition: 4th
Copyright year: 2006
Publisher: Brooks/Cole
Publication date: 11/11/2005
Binding: Hardcover
Pages: 871
Size: 9.00" wide x 11.25" long x 1.50" tall
Weight: 4.4
Language: English

Jack Gilbert joined the faculty of the University of Texas at Austin in 1965 and moved to Santa Clara University in 2007, where he is Professor of Chemistry & Biochemistry. He received the Advisory Council Teaching Excellence Award at UT the 2002-2003 academic year, as well as many other recognitions in teaching. While at UT, he co-authored several editions of the first laboratory textbook in organic chemistry that emphasized reactions mechanisms, as well as laboratory techniques, including spectroscopy. He continues to update the textbook, now with the able assistance of Steve Martin.

Stephen Martin received his B. S. degree in chemistry from the University of New Mexico in 1968 and his Ph.D. degree from Princeton University in 1972. After postdoctoral years at the University of Munich and MIT, he joined the faculty at The University of Texas at Austin in 1974, where he currently holds the M. June and J. Virgil Waggoner Regents Chair in Chemistry. His research interests lie broadly in organic and bioorganic chemistry. In the former area, his endeavors involve developing and applying new methods and strategies to the syntheses of biologically active natural and non-natural products, especially those containing nitrogen and oxygen heterocyclic subunits. In the biological…    

Introduction, Record Keeping, and Laboratory Safety
Techniques and Apparatus
Solids: Recrystallization and Melting Points
Liquids: Distillation and Boiling Points
Extraction
Chromatography
Stereoisomers
Spectral Methods
Alkanes
Alkenes
Alkynes
Dienes: The Diels-Alder Reaction
Kinetic and Thermodynamic Control of a Reaction
Nucleophilic Aliphatic Substitution: Preparation for Alkyl Halides
Electrophilic Aromatic Substitution
Oxidation of Alcohols and Carbonyl Compounds
Reduction Reactions of Double Bonds: Alkenes, Carbonyl Compounds, and Imines
Reactions of Carbonyl Compounds
Organometallic Chemistry
Carboxylic Acids and Their Derivatives
Multistep Organic Synthesis
Polymers
Carbohydrates
?-Amino Acids and Peptides
Identifying Organic Compounds
The Literature of Organic Chemistry.