Spectrometric Identification of Organic Compounds

ISBN-10: 0471393622

ISBN-13: 9780471393627

Edition: 7th 2005 (Revised)

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Description: This classic text's goal remains the same: to be a 'how to, hands on, self-sufficient teaching manual', based on the concept that organic compounds can be identified by the synergistic information obtained from MR, IR & NMR spectrometry.

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Book details

List price: $248.95
Edition: 7th
Copyright year: 2005
Publisher: John Wiley & Sons, Incorporated
Publication date: 1/14/2005
Binding: Hardcover
Pages: 512
Size: 9.00" wide x 11.50" long x 1.00" tall
Weight: 2.332
Language: English

Mass Spectrometry
Introduction
Instrumentation
Ionization Methods
Mass Analyzers
Interpretation of El Mass Spectra
Mass Spectra of Some Chemical Classes
Infrared Spectrometry
Introduction
Theory
Instrumentation
Sample Handling
Interpretations of Spectra
Characteristic Group Absorption of Organic Molecules
Proton Magnetic Resonance Spectrometry
Introduction
Theory
Instrumentation and Sample Handling
Chemical Shift
Spin Coupling, Multiplets, Spin Systems
Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons
Coupling of Protons to Other Important Nuclei ( 19 F, E, 31 P, 29 Si, and 13 C
Chemical Shift Equivalence
Magnetic Equivalence (Spin-Coupling Equivalence)
AMX, ABX, and ABC Rigid Systems with Three Coupling Constants
Confirmationally Mobile, Open-Chain Systems. Virtual Coupling
Chirality
Vicinal and Geminal Coupling
Low-Range Coupling
Selective Spin Decoupling. Double Resonance
Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space
Carbon-13 NMR Spectrometry
Introduction
Theory
Interpretation of a Simple 13 C Spectrum: Diethyl Phthalate
Quantitative 13 C Analysis
Chemical Shift Equivalence
DEPT
Chemical Classes and Chemical Shifts
Correlation NMR Spectrometry; 2-D NMR
Introduction
Theory
Correlation Spectrometry
Ipsenol: 1 H- 1 H COSY
Caryophyllene Oxide
13 C- 13 C Correlations: Inadequate
Lactose
Relayed Coherence Transfer: TOCSY
HMQC - TOCSY
ROESY
VGSE
Gradient Field NMR
NMR Spectrometry of Other Important Spin 1/2 Nuclei
Introduction
15 N Nuclear Magnetic Resonance
19 F Nuclear Magnetic Resonance
29 Si Nuclear Magnetic Resonance
31 P Nuclear Magnetic Resonance
Conclusion
Solved Problems
Introduction
Assigned Problems
Introduction
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