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Foreword to the first English edition | |
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Preface to the first English edition | |
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Preface to second edition | |
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Acknowledgments | |
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Introduction | |
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Separation Methods | |
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General aspects of chromatography | |
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General concepts of analytical chromatography | |
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The chromatogram | |
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Gaussian-shaped elution peaks | |
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The plate theory | |
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Nernst partition coefficient (K) | |
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Column efficiency | |
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Retention parameters | |
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Separation (or selectivity) factor between two solutes | |
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Resolution factor between two peaks | |
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The rate theory of chromatography | |
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Optimization of a chromatographic analysis | |
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Classification of chromatographic techniques | |
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Problems 2 | |
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Components of a GC installation | |
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Carrier gas and flow regulation | |
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Sample introduction and the injection chamber | |
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Thermostatically controlled oven | |
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Columns | |
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Stationary phases | |
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Principal gas chromatographic detectors | |
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Detectors providing structural data | |
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Fast chromatography | |
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Multi-dimensional chromatography | |
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Retention indexes and stationary phase constants | |
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High-performance liquid chromatography | |
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The beginnings of HPLC | |
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General concept of an HPLC system | |
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Pumps and gradient elution | |
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Injectors | |
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Columns | |
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Stationary phases | |
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Chiral chromatography | |
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Mobile phases | |
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Paired-ion chromatography | |
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Hydrophobic interaction chromatography | |
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Principal detectors | |
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Evolution and applications of HPLC | |
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Ion chromatography | |
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Basics of ion chromatography | |
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Stationary phases | |
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Mobile phases | |
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Conductivity detectors | |
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Ion suppressors | |
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Principle and basic relationship | |
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Areas of the peaks and data treatment software | |
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External standard method | |
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Internal standard method | |
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Internal normalization method | |
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Thin layer chromatography | |
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Principle of TLC | |
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Characteristics of TLC | |
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Stationary phases | |
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Separation and retention parameters | |
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Quantitative TLC | |
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Supercritical fluid chromatography | |
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Supercritical fluids: a reminder | |
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Supercritical fluids as mobile phases | |
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Instrumentation in SFC | |
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Comparison of SFC with HPLC and GC | |
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SFC in chromatographic techniques | |
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Size exclusion chromatography | |
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Principle of SEC | |
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Stationary and mobile phases | |
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Calibration curves | |
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Instrumentation | |
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Applications of SEC | |
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Capillary electrophoresis and electrochromatography | |
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From zone electrophoresis to capillary electrophoresis | |
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Electrophoretic mobility and electro-osmotic flow | |
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Instrumentation | |
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Electrophoretic techniques | |
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Performance of CE | |
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Capillary electrochromatography | |
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Problems | |
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Spectroscopic Methods | |
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Ultraviolet and visible absorption spectroscopy | |
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The UV/Vis spectral region and the origin of the absorptions | |
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The UV/Vis spectrum | |
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Electronic transitions of organic compounds | |
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Chromophore groups | |
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Solvent effects: solvatochromism | |
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Fieser-Woodward rules | |
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Instrumentation in the UV/Visible | |
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UV/Vis spectrophotometers | |
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Quantitative analysis | |