Chemical Analysis Modern Instrumentation Methods and Techniques

ISBN-10: 0470859032

ISBN-13: 9780470859032

Edition: 2nd 2005 (Revised)

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Description:

Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail.Provides a thorough introduction to a wide range of the most important and widely used instrumental techniquesMaintains a careful balance between depth and breadth of coverageIncludes examples, problems and their solutionsIncludes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis
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Book details

List price: $76.00
Edition: 2nd
Copyright year: 2005
Publisher: John Wiley & Sons, Incorporated
Publication date: 5/7/2007
Binding: Paperback
Pages: 600
Size: 6.75" wide x 9.50" long x 1.50" tall
Weight: 2.486
Language: English

Foreword to the first English edition
Preface to the first English edition
Preface to second edition
Acknowledgments
Introduction
Separation Methods
General aspects of chromatography
General concepts of analytical chromatography
The chromatogram
Gaussian-shaped elution peaks
The plate theory
Nernst partition coefficient (K)
Column efficiency
Retention parameters
Separation (or selectivity) factor between two solutes
Resolution factor between two peaks
The rate theory of chromatography
Optimization of a chromatographic analysis
Classification of chromatographic techniques
Problems 2
Components of a GC installation
Carrier gas and flow regulation
Sample introduction and the injection chamber
Thermostatically controlled oven
Columns
Stationary phases
Principal gas chromatographic detectors
Detectors providing structural data
Fast chromatography
Multi-dimensional chromatography
Retention indexes and stationary phase constants
High-performance liquid chromatography
The beginnings of HPLC
General concept of an HPLC system
Pumps and gradient elution
Injectors
Columns
Stationary phases
Chiral chromatography
Mobile phases
Paired-ion chromatography
Hydrophobic interaction chromatography
Principal detectors
Evolution and applications of HPLC
Ion chromatography
Basics of ion chromatography
Stationary phases
Mobile phases
Conductivity detectors
Ion suppressors
Principle and basic relationship
Areas of the peaks and data treatment software
External standard method
Internal standard method
Internal normalization method
Thin layer chromatography
Principle of TLC
Characteristics of TLC
Stationary phases
Separation and retention parameters
Quantitative TLC
Supercritical fluid chromatography
Supercritical fluids: a reminder
Supercritical fluids as mobile phases
Instrumentation in SFC
Comparison of SFC with HPLC and GC
SFC in chromatographic techniques
Size exclusion chromatography
Principle of SEC
Stationary and mobile phases
Calibration curves
Instrumentation
Applications of SEC
Capillary electrophoresis and electrochromatography
From zone electrophoresis to capillary electrophoresis
Electrophoretic mobility and electro-osmotic flow
Instrumentation
Electrophoretic techniques
Performance of CE
Capillary electrochromatography
Problems
Spectroscopic Methods
Ultraviolet and visible absorption spectroscopy
The UV/Vis spectral region and the origin of the absorptions
The UV/Vis spectrum
Electronic transitions of organic compounds
Chromophore groups
Solvent effects: solvatochromism
Fieser-Woodward rules
Instrumentation in the UV/Visible
UV/Vis spectrophotometers
Quantitative analysis
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