| |
| |
Preface to the Second Edition | |
| |
| |
Preface | |
| |
| |
Acknowledgments | |
| |
| |
| |
Introduction | |
| |
| |
A Brief History | |
| |
| |
Definitions | |
| |
| |
Overview: Advantages and Disadvantages | |
| |
| |
Instrumentation | |
| |
| |
References | |
| |
| |
| |
Instrument Overview | |
| |
| |
Carrier Gas | |
| |
| |
Flow Control and Measurement | |
| |
| |
Sample Inlets and Sampling Devices | |
| |
| |
Columns | |
| |
| |
Temperature Zones | |
| |
| |
Detectors | |
| |
| |
Data Systems | |
| |
| |
References | |
| |
| |
| |
Basic Concepts and Terms | |
| |
| |
Definitions, Terms, and Symbols | |
| |
| |
The Rate Theory | |
| |
| |
A Redefinition of H | |
| |
| |
The Achievement of Separation | |
| |
| |
References | |
| |
| |
| |
Stationary Phases | |
| |
| |
Selecting a Column | |
| |
| |
Classification of Stationary Phases for GLC | |
| |
| |
Liquid Stationary Phases (GLC) | |
| |
| |
Solid Stationary Phases (GSC) | |
| |
| |
References | |
| |
| |
| |
Packed Columns and Inlets | |
| |
| |
Solid Supports | |
| |
| |
Liquid Stationary Phases | |
| |
| |
Solid Stationary Phases (GSC) | |
| |
| |
Gas Analysis | |
| |
| |
Analysis of Other Inorganics | |
| |
| |
Inlets for Liquid Samples and Solutions | |
| |
| |
Special Columns | |
| |
| |
Upgrading for Capillary Columns | |
| |
| |
References | |
| |
| |
| |
Capillary Columns and Inlets | |
| |
| |
Types of OT Columns | |
| |
| |
OT Column Tubing | |
| |
| |
Advantages of OT Columns | |
| |
| |
Column Selection | |
| |
| |
Capillary Inlet Systems | |
| |
| |
Miscellaneous Topics | |
| |
| |
References | |
| |
| |
| |
Detectors | |
| |
| |
Classification of Detectors | |
| |
| |
Detector Characteristics | |
| |
| |
Flame Ionization Detector (FID) | |
| |
| |
Thermal Conductivity Detector (TCD) | |
| |
| |
Electron Capture Detector (ECD) | |
| |
| |
Other Detectors | |
| |
| |
References | |
| |
| |
| |
Qualitative and Quantitative Analysis | |
| |
| |
Qualitative Analysis | |
| |
| |
Quantitative Analysis | |
| |
| |
References | |
| |
| |
| |
Programmed Temperature | |
| |
| |
Temperature Effects | |
| |
| |
Advantages and Disadvantages of PTGC | |
| |
| |
Requirements of PTGC | |
| |
| |
Theory of PTGC | |
| |
| |
Special Topics | |
| |
| |
References | |
| |
| |
| |
Gas Chromatography-Mass Spectrometry (GC-MS) | |
| |
| |
Instrumentation | |
| |
| |
History | |
| |
| |
Limitations of GC-MS Systems | |
| |
| |
Data Analysis | |
| |
| |
References | |
| |
| |
| |
Multidimensional Gas Chromatography | |
| |
| |
Overview | |
| |
| |
Fundamental Principles of Multidimensional Chromatography | |
| |
| |
GC�GC with Heart Cutting | |
| |
| |
Comprehensive GC�GC | |
| |
| |
LC�GC with Heart Cutting | |
| |
| |
Comprehensive LC�GC | |
| |
| |
Summary | |
| |
| |
References | |
| |
| |
| |
Sampling Methods | |
| |
| |
Overview | |
| |
| |
Liquid-Liquid Extraction (LLE) | |
| |
| |
Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE) | |
| |
| |
Liquid-Solid Extraction: Solid-Phase Extraction (SPE) | |
| |
| |
Liquid- or Solid-Vapor Extraction: Headspace Extraction | |
| |
| |
Solid-Phase Micro-extraction (SPME) | |
| |
| |
Additional Techniques and Summary | |
| |
| |
References | |
| |
| |
| |
Special Topics | |
| |
| |
Fast GC | |
| |
| |
Chiral Analysis by GC | |
| |
| |
GC Analysis of Nonvolatile Compounds | |
| |
| |
References | |
| |
| |
| |
Troubleshooting GC Systems | |
| |
| |
| |
Symbols and Acronyms | |
| |
| |
| |
Guidelines for Selecting Capillary Columns | |
| |
| |
| |
GC: How to Avoid Problems | |
| |
| |
| |
Calculation of Split Ratio for Split Injection on OT Columns | |
| |
| |
| |
Operating Conditions for Capillary Columns | |
| |
| |
| |
OV Liquid Phases Physical Property Data | |
| |
| |
| |
Some Compressibility Correction Factors (J) | |
| |
| |
| |
Some Internet Websites for Gas Chromatographers | |
| |
| |
| |
Other Books on Gas Chromatography | |
| |
| |
Index of Applications | |
| |
| |
Index | |