Multiscale Operational Organic Chemistry A Problem Solving Approach to the Laboratory

ISBN-10: 0132413752
ISBN-13: 9780132413756
Edition: 2nd 2009
Authors: John W. Lehman
List price: $195.00 Buy it from $61.85 Rent it from $31.52
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Description: This comprehensive lab companion provides enough theory to help readers understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. Makes substantive  More...

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Book details

List price: $195.00
Edition: 2nd
Copyright year: 2009
Publisher: Prentice Hall PTR
Publication date: 4/9/2008
Binding: Hardcover
Pages: 984
Size: 8.00" wide x 9.75" long x 1.25" tall
Weight: 4.048
Language: English

This comprehensive lab companion provides enough theory to help readers understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. Makes substantive revisions of many operations to clarify existing material and add new information. Emphasizes environmentally friendly (i.e. ldquo;greenrdquo;) lab experiments. Adds a new section on Chemistry and the Environment. A useful guide for chemists and other professionals who do laboratory work in the scientific fields.

Please note this is the 1st edition Table of Contents
Preface
Introduction
MASTERING THE OPERATIONS
Learning Basic Operations
The Effect of pH on a Food Preservative
Extraction and Evaporation
Separating the Components of ldquo;Panacetin.rdquo;
Recrystallization and Melting-Point Measurement
Identifying a Constituent of ldquo;Panacetin.rdquo;
Heating under Reflux
Synthesis of Salicylic Acid from Wintergreen Oil
Simple Distillation, Gas Chromatography
Preparation of Synthetic Banana Oil
Fractional Distillation
Separation of Petroleum Hydrocarbons
Addition, Mixing, Sublimation
Preparation of Camphor
Boiling Point, Refractive Index
Identification of a Petroleum Hydrocarbon
Column Chromatography, UV-VIS Spectrometry
Isolation and Isomerization of Lycopene from Tomato Paste
Steam Distillation, Infrared Spectrometry
Isolation and Identification of the Major Constituent of Clove Oil
Thin-Layer Chromatography, NMR Spectrometry
Identification of Unknown Ketones
Vacuum Distillation, Optical Rotation
Optical Activity of hellip;a-Pinene
Correlated Laboratory Experiments
Investigation of a Chemical Bond by Infrared Spectrometry
Properties of Common Functional Groups
Thin-Layer Chromatographic Analysis of Drug Components
Separation of an Alkane Clathrate
Isomers and Isomerization Reactions
Structures and Properties of Stereoisomers
Bridgehead Reactivity in an S n 1 Solvolysis Reaction
Reaction of Iodoetane with Saccharin, an Ambident Nucleophile
Dehydration of Methylcyclohexanols
Synthesis of 7,7-Dichloronorcarane Using a Phase-Transfer Catalyst
Stereochemistry of the Addition of Bromine totrans-Cinnamic Acid
Preparation of Bromotriphenylmethane and the Trityl Free Radical
Chain-Growth Polymerization of Styrene and Methyl Methacrylate
Synthesis of Ethanol by Fermentation
Reaction of Butanols with Hydrobromic Acid
Borohydride Reduction of Vanillin to Vanillyl Alcohol
Synthesis of Triphenylmethanol and the Trityl Carbocation
Identification of a Conjugated Diene from Eucalyptus Oil
Spectral Identification of Terpenoids
Synthesis

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