Organic Structure Determination Using 2-D NMR Spectroscopy A Problem-Based Approach

ISBN-10: 0123849705

ISBN-13: 9780123849700

Edition: 2nd 2012

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Description: This book contains 30-40 quality 2D NMR data sets following an introductory section describing the methodology employed. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges at the present time are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.. Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra. Contains 20 known and 20 unknown structure determination problems. Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

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Book details

List price: $69.95
Edition: 2nd
Copyright year: 2012
Publisher: Elsevier Science & Technology Books
Publication date: 12/30/2011
Binding: Paperback
Pages: 540
Size: 7.50" wide x 9.25" long x 1.25" tall
Weight: 2.904
Language: English

Background and Methods
Introduction
Instrumental Considerations
Data Collection, Processing, and Plotting
1H and 13C Chemical Shifts
Symmetry and Topicity
Through-Bond Effects: Spin-Spin (J) Coupling
Through-Space Effects: the Nuclear Overhauser Effect (NOE)
Molecular Dynamics
Strategies for Assigning Molecules
Strategies for Elucidating Unknown Molecular Structures
Problems
Simple Assignment Problems
Complex Assignment Problems
Simple Unknown Problems
Complex Unknown Problems
NMR Resonance Assignment Problems
NMR Unknown Problems
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